TA Instruments

Sachainchi desengrasada 12%-0042f

23/05/2022 12:45:09 p. m.

Sample name	Sachainchi desengrasada 12%
Sample notes	 
Experiment notes	
Operator	
Sample density	1,000 g/cm^3
Results file name	Sachainchi desengrasada 12%
Run number	42 
Results directory	C:\Ta\Data\Ar1500\Ar1500\DIEGO ROA
Experiment was run on	23/05/2022 12:45:09 p. m.

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	25,0 C
Wait for correct temperature	No
Do set temperature	Yes
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:02:00 hh:mm:ss
Wait for zero velocity	No
Purge gas only	No

Step name	Stepped flow step 1
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000E-3 1/s
End controlled variable	shear rate 0,01000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 2
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,01000 1/s
End controlled variable	shear rate 0,1000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 3
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,1000 1/s
End controlled variable	shear rate 1,000 1/s
Ramp mode	log 
Points per decade	5 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 4
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000 1/s
End controlled variable	shear rate 100,0 1/s
Ramp mode	log 
Points per decade	8 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Conditioning Step 2
Step notes	
Perform step	Yes
Initial temperature	25,0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Perform pre-shear	Yes
Pre-shear variable	10,00 1/s
Pre-shear duration	0:00:10 hh:mm:ss
Motor mode	auto 
Perform equilibration	Yes
Equilibration duration	0:02:00 hh:mm:ss
Wait for zero velocity	No
Purge gas only	No

Step name	Temperature ramp step 1
Step notes	
Perform step	Yes
Ramp type	Temperature ramp
Start temperature	25,0 C
End temperature	90,0 C
Wait for start temperature	Yes
Ramp rate	10,00 C/min
Delay time	0:00:09 hh:mm:ss
Controlled variable	shear rate 10,00 1/s
Motor mode	auto 

Step name	Temperature ramp step 2
Step notes	
Perform step	Yes
Ramp type	Temperature ramp
Start temperature	90,0 C
End temperature	90,0 C
Wait for start temperature	No
Ramp duration	0:05:00 hh:mm:ss
Delay time	0:00:09 hh:mm:ss
Controlled variable	shear rate 10,00 1/s
Motor mode	auto 

Step name	Temperature ramp step 3
Step notes	
Perform step	Yes
Ramp type	Temperature ramp
Start temperature	90,0 C
End temperature	25,0 C
Wait for start temperature	No
Ramp rate	10,00 C/min
Delay time	0:00:09 hh:mm:ss
Controlled variable	shear rate 10,00 1/s
Motor mode	auto 

Step name	Conditioning Step 3
Step notes	
Perform step	Yes
Initial temperature	25,0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Perform pre-shear	Yes
Pre-shear variable	1,000 1/s
Pre-shear duration	0:00:10 hh:mm:ss
Motor mode	auto 
Perform equilibration	Yes
Equilibration duration	0:02:00 hh:mm:ss
Wait for zero velocity	No
Purge gas only	No

Step name	Stepped flow step 5
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000E-3 1/s
End controlled variable	shear rate 0,01000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 6
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,01000 1/s
End controlled variable	shear rate 0,1000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 7
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,1000 1/s
End controlled variable	shear rate 1,000 1/s
Ramp mode	log 
Points per decade	5 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 8
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000 1/s
End controlled variable	shear rate 100,0 1/s
Ramp mode	log 
Points per decade	8 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	No
Set temperature system idle	No

Geometry name	Starch cell
Geometry notes	Starch cell
Geometry material	High temperature
gap	5500 micro m
Calibration factor	10800 
Gap offset	0 micro m
Geometry inertia	2,245 micro N.m.s^2
Shear rate factor	1,000 
Shear stress factor	10800 1/m^3
Measurement system factor	10800 1/m^3
Fluid density factor	1,000E-15 m^5
Normal force factor	1,000 1/m^2
Backoff distance	1,25E5 micro m

Gap zero mode	Standard
Sample compression	none 
Compression distance	1000,0 micro m
Compression velocity	100,0 micro m/s
Fine velocity	1000,0 micro m/s
Coarse velocity	3000,0 micro m/s
Other velocity	3000,0 micro m/s
Current temperature system	Starch cell
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	5,0 C
Cooling water range	15,0 C
Bearing friction correction	Yes
Bearing friction	1,222 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1,0000 , offset 0 C
	Water bath - span 1,0000 , offset 0 C
	Torsion oven - plate - span 1,0000 , offset 0 C
	Torsion oven - solid sample - span 1,0000 , offset 0 C
	Peltier concentric cylinders - span 1,0000 , offset 0 C
	None - span 1,0000 , offset 0 C
	Stress relaxation - span 1,0000 , offset 0 C
	Current temperature system - span 1,0000 , offset 0 C
Bearing mapping type	standard 
Number of mapping iterations	1
Instrument type (MType)	AR1500ex
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	172.23.191.2
Software version	V5.8.2
Windows version	Windows XP 6.2
Instrument inertia	15,97 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0,2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0,1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	3,000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	No
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	No
Creep zero displacement	Yes
Store images to the results for creep steps	No
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	No
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	No
Flow torque limit	10,00 micro N.m
Flow velocity limit	1,000E-3 rad/s
Oscillation torque limit	5,00 micro N.m
Oscillation displacement limit	1,00E-5 rad
Oscillation raw phase limit	170,0 degrees
Oscillation minimum normal force limit	0 N
Oscillation maximum normal force limit	0 N
Flow velocity tolerance	5,00 %
Oscillation torque tolerance	1,00 %
Oscillation displacement tolerance	5,00 %
Oscillation velocity tolerance	5,00 %
Temperature tolerance	1,0 C

Stepped flow step 1

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,1718	1,008E-3	170,5	9,9540	28,0	0
0,6025	2,153E-3	279,8	20,016	28,0	0
1,153	4,639E-3	248,6	30,157	28,0	0
2,108	9,996E-3	210,9	40,250	28,0	0

Stepped flow step 2

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

2,991	9,997E-3	299,2	9,9690	28,0	0
4,569	0,02154	212,1	20,094	28,0	0
6,978	0,04642	150,3	30,172	28,1	0
8,002	0,1000	80,01	40,266	28,1	0
6,741	0,1000	67,40	50,313	28,1	0

Stepped flow step 3

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

6,368	0,1000	63,68	9,9380	28,1	0
5,965	0,1585	37,64	20,031	28,1	0
4,766	0,2512	18,98	30,063	28,1	0
3,476	0,3981	8,730	40,141	28,1	0
2,488	0,6310	3,943	50,219	28,1	0
1,709	1,000	1,709	60,281	28,1	0

Stepped flow step 4

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

1,410	1,000	1,410	9,9840	28,1	0
1,094	1,334	0,8205	20,016	28,1	0
0,9398	1,778	0,5285	30,078	28,1	0
0,8677	2,371	0,3659	40,156	28,1	0
0,8786	3,162	0,2778	50,234	28,1	0
0,8976	4,217	0,2129	60,359	28,1	0
1,008	5,623	0,1792	70,453	28,2	0
1,165	7,499	0,1554	80,484	28,2	0
1,498	10,00	0,1498	90,578	28,2	0
2,071	13,33	0,1553	100,72	28,2	0
2,769	17,78	0,1557	110,73	28,2	0
3,472	23,71	0,1464	120,84	28,2	0
4,484	31,62	0,1418	131,16	28,2	0
6,140	42,17	0,1456	141,23	28,2	0
8,443	56,23	0,1501	151,33	28,2	0
11,20	74,99	0,1494	161,61	28,3	0
14,11	100,0	0,1411	171,69	28,3	0

Temperature ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

1,074	10,00	0,1074	8,9960	24,9	0
1,073	10,00	0,1073	18,004	25,3	0
1,068	10,00	0,1068	27,000	26,3	0
1,056	10,00	0,1056	36,008	27,9	0
1,032	10,00	0,1032	45,020	29,8	0
1,005	9,999	0,1005	54,008	31,6	0
0,9899	10,00	0,09899	62,996	33,2	0
0,9708	10,00	0,09708	72,008	34,7	0
0,9422	10,00	0,09422	81,008	36,4	0
0,9212	10,00	0,09211	90,020	38,0	0
0,9098	10,00	0,09099	99,012	39,6	0
0,9040	10,00	0,09040	108,01	41,2	0
0,8939	10,00	0,08939	117,00	42,8	0
0,8898	10,00	0,08898	126,00	44,3	0
0,8822	10,00	0,08822	135,02	45,8	0
0,8912	10,00	0,08912	144,01	47,3	0
0,8844	10,00	0,08844	153,01	48,8	0
0,8786	10,00	0,08786	162,02	50,3	0
0,8957	10,00	0,08957	171,01	51,8	0
0,9134	10,00	0,09134	180,00	53,3	0
0,9312	10,00	0,09312	189,00	54,8	0
0,9583	9,999	0,09583	198,00	56,3	0
0,9705	10,00	0,09704	207,01	57,8	0
0,9929	10,00	0,09930	216,00	59,3	0
1,001	10,00	0,1001	225,01	60,8	0
1,005	10,00	0,1005	234,00	62,3	0
1,013	10,00	0,1013	243,00	63,8	0
1,020	10,00	0,1020	252,00	65,4	0
1,023	10,00	0,1023	261,02	66,8	0
1,037	10,00	0,1037	270,00	68,3	0
1,077	10,00	0,1077	279,02	69,8	0
1,137	10,00	0,1138	288,00	71,3	0
1,233	10,00	0,1233	297,02	72,9	0
1,431	10,00	0,1431	306,00	74,4	0
1,796	10,00	0,1796	315,00	75,9	0
2,434	10,00	0,2433	324,02	77,5	0
3,281	10,00	0,3281	333,01	78,9	0
4,396	10,00	0,4395	342,00	80,4	0
5,587	10,00	0,5586	351,00	81,8	0
6,158	9,998	0,6159	360,00	83,3	0
5,960	9,999	0,5961	369,00	84,8	0

Temperature ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

5,373	9,999	0,5373	8,9920	86,4	0
5,337	10,00	0,5337	17,992	88,6	0
6,891	9,999	0,6891	27,000	90,5	0
7,294	10,00	0,7294	36,004	91,5	0
7,594	9,999	0,7595	45,004	91,9	0
6,875	9,999	0,6876	54,004	90,7	0
5,862	10,00	0,5862	62,996	89,3	0
5,230	10,00	0,5230	72,012	89,2	0
4,742	10,00	0,4742	81,000	89,8	0
4,512	10,00	0,4512	90,000	90,5	0
4,314	9,999	0,4314	99,008	90,8	0
4,374	10,00	0,4374	107,99	90,9	0
4,457	9,999	0,4458	117,00	90,9	0
4,450	10,00	0,4450	126,01	90,8	0
4,481	9,999	0,4482	135,00	90,6	0
4,459	10,00	0,4459	144,00	90,5	0
4,506	9,999	0,4506	153,01	90,4	0
4,446	10,00	0,4446	162,00	90,3	0
4,437	10,00	0,4437	171,00	90,2	0
4,449	9,999	0,4449	180,01	90,1	0
4,414	10,00	0,4414	189,00	90,0	0
4,405	10,00	0,4405	198,01	90,0	0
4,421	9,999	0,4422	207,00	90,0	0
4,376	10,00	0,4375	215,99	90,1	0
4,375	10,00	0,4375	225,00	90,0	0
4,399	10,00	0,4399	234,00	90,0	0
4,384	10,00	0,4384	242,99	90,0	0
4,366	10,00	0,4366	252,01	90,0	0
4,363	9,999	0,4363	261,00	90,0	0
4,319	10,00	0,4319	270,01	90,0	0
4,338	10,00	0,4338	279,00	90,0	0

Temperature ramp step 3

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

4,352	10,00	0,4352	9,0040	90,0	0
4,355	10,00	0,4355	18,004	89,5	0
4,565	10,00	0,4564	27,004	87,0	0
4,831	10,00	0,4831	36,004	85,4	0
5,060	10,00	0,5060	45,004	84,5	0
5,161	9,999	0,5162	54,012	83,5	0
5,426	10,00	0,5426	63,000	81,8	0
5,550	10,00	0,5549	72,004	79,8	0
5,679	10,00	0,5679	81,004	78,6	0
5,810	10,00	0,5810	90,008	77,3	0
5,910	10,00	0,5910	99,008	75,1	0
5,904	10,00	0,5904	108,02	73,9	0
6,046	9,999	0,6046	117,00	72,7	0
6,183	9,999	0,6183	126,00	70,6	0
6,178	10,00	0,6178	135,01	69,3	0
6,310	10,00	0,6310	144,01	68,0	0
6,491	9,999	0,6492	153,00	66,1	0
6,525	9,999	0,6526	162,00	64,8	0
6,711	10,00	0,6711	171,01	63,3	0
6,759	9,999	0,6760	180,00	61,6	0
7,010	10,00	0,7010	189,01	60,3	0
7,117	9,998	0,7118	198,00	58,7	0
7,358	10,00	0,7358	207,00	57,2	0
7,571	10,00	0,7570	216,02	55,7	0
7,856	10,00	0,7856	225,00	54,2	0
8,080	9,999	0,8081	234,01	52,7	0
8,254	9,999	0,8255	243,01	51,3	0
8,569	10,00	0,8569	252,01	49,7	0
8,757	10,00	0,8756	260,99	48,2	0
9,097	10,00	0,9096	270,01	46,8	0
9,384	9,999	0,9385	279,01	45,3	0
9,744	10,00	0,9743	288,01	43,8	0
10,20	10,00	1,020	297,00	42,3	0
10,43	9,996	1,043	306,00	40,9	0
10,81	10,00	1,081	315,00	39,3	0
11,02	9,997	1,103	324,00	37,9	0
11,46	9,997	1,146	333,01	36,5	0
11,62	10,00	1,162	342,00	35,0	0
11,78	9,997	1,179	351,01	33,6	0
12,27	9,998	1,228	360,00	32,4	0
12,45	9,998	1,245	369,00	31,2	0

Stepped flow step 5

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,6350	1,002E-3	633,9	9,9690	24,9	0
1,362	2,150E-3	633,3	20,016	25,0	0
2,890	4,634E-3	623,6	30,078	25,0	0
6,081	9,994E-3	608,4	40,141	25,0	0

Stepped flow step 6

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

7,867	9,994E-3	787,2	9,9380	25,0	0
11,20	0,02153	520,0	20,032	25,0	0
14,48	0,04642	311,8	30,110	25,0	0
14,69	0,09999	146,9	40,172	24,9	0
16,51	0,1000	165,1	50,250	24,9	0

Stepped flow step 7

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

13,91	0,09998	139,1	9,9850	24,9	0
15,47	0,1585	97,59	20,063	25,0	0
15,66	0,2512	62,35	30,079	25,0	0
14,82	0,3981	37,23	40,172	25,0	0
13,91	0,6310	22,05	50,250	25,0	0
13,94	1,000	13,94	60,297	25,0	0

Stepped flow step 8

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

14,03	1,000	14,03	9,9850	25,0	0
13,79	1,333	10,34	20,094	25,0	0
13,93	1,778	7,831	30,141	25,0	0
13,80	2,371	5,821	40,203	25,0	0
13,81	3,162	4,367	50,282	25,0	0
14,06	4,217	3,334	60,375	25,0	0
14,41	5,623	2,563	70,438	25,0	0
14,38	7,499	1,918	80,485	25,0	0
14,44	10,00	1,444	90,578	25,0	0
14,60	13,34	1,095	100,64	25,0	0
14,88	17,78	0,8370	110,72	25,0	0
15,39	23,71	0,6490	120,74	25,0	0
16,16	31,62	0,5110	130,83	25,0	0
17,37	42,17	0,4118	140,89	25,0	0
18,91	56,23	0,3362	150,97	25,0	0
25,87	74,99	0,3450	161,02	25,0	0
30,23	100,0	0,3023	171,09	25,0	0

